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Calcareous nannofossils assemblages for provenance analysis of European paintings: From the sample preparation to the assemblage comparison
Jaques, Victory Armida Janine ; Holcová, Katarína (advisor) ; Caruso, Francesco (referee) ; Oszczypko-Ciowes, Marta (referee)
This PhD thesis is a commentary of four studies published and a fifth study submitted in peer reviewed and impacted scientific journals. Three studies are methodological work for the preparation of painted micro-samples to improve the measurements accuracy, the samples visualisation, and the combination of measurements methods. The two other papers focus on the fossil assemblages determination and comparison between reference historical areas and original paintings. This work is divided into three main parts, namely the introduction, the methods, and the calcareous nannofossils assemblages. In the introduction, detailed explanations are given about the paintings, historical materials, trade roads, what are nannofossils, how and why to use them. In the methods section, developed preparatory methodologies are summarised, and the most important results are explained. In the third part, the nannofossils assemblages, the differences between the assemblages from different areas in Europe compared to original paintings are explained and correlated to the literature. The impact of the preparatory methods on the results is discussed, and a conclusion is drawn from it in the context of painted artefacts in the Cultural Heritage field are unique, and so are the micro-samples from them. To extract most...
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Study of cooperative dislocation phenomena in solids by the acoustic emission technique
Knapek, Michal ; Chmelík, František (advisor) ; Haušild, Petr (referee) ; Landa, Michal (referee)
Title: Study of cooperative dislocation phenomena in solids by the acoustic emis- sion technique Author: Michal KNAPEK Department: Department of Physics of Materials Supervisor: doc. RNDr. František Chmelík, CSc., Department of Physics of Materials Abstract: Plastic deformation of micron-scale crystalline materials differs con- siderably from bulk specimens, as it is characterized by random strain bursts. Three categories of metallic samples were investigated in this thesis: micron- scale copper micropillars with varied geometries, submillimeter-scale aluminum microwires, and aluminum and aluminum-magnesium salt-replicated foams. Very precise fabrication methods and sensitive measurement set-ups consisting of uni- axial compression and tensile tests with concurrent acoustic emission (AE) record- ing were developed. These fine methods allowed for investigations of effects re- lated to plastic deformation at micrometer scales, i.e. the dislocation dynamics associated with the stress drops. Size effects in plastic deformation, as well as clear correlations between the stress drops and the AE events, were found in mi- crosamples, confirming that dislocation avalanches are indeed responsible for the stochastic character of deformation processes also at microscales. Open-cell pure aluminum and aluminum-magnesium...
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Study of cooperative dislocation phenomena in solids by the acoustic emission technique
Knapek, Michal ; Chmelík, František (advisor)
Title: Study of cooperative dislocation phenomena in solids by the acoustic emis- sion technique Author: Michal KNAPEK Department: Department of Physics of Materials Supervisor: doc. RNDr. František Chmelík, CSc., Department of Physics of Materials Abstract: Plastic deformation of micron-scale crystalline materials differs con- siderably from bulk specimens, as it is characterized by random strain bursts. Three categories of metallic samples were investigated in this thesis: micron- scale copper micropillars with varied geometries, submillimeter-scale aluminum microwires, and aluminum and aluminum-magnesium salt-replicated foams. Very precise fabrication methods and sensitive measurement set-ups consisting of uni- axial compression and tensile tests with concurrent acoustic emission (AE) record- ing were developed. These fine methods allowed for investigations of effects re- lated to plastic deformation at micrometer scales, i.e. the dislocation dynamics associated with the stress drops. Size effects in plastic deformation, as well as clear correlations between the stress drops and the AE events, were found in mi- crosamples, confirming that dislocation avalanches are indeed responsible for the stochastic character of deformation processes also at microscales. Open-cell pure aluminum and aluminum-magnesium...
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Study of cooperative dislocation phenomena in solids by the acoustic emission technique
Knapek, Michal ; Chmelík, František (advisor) ; Haušild, Petr (referee) ; Landa, Michal (referee)
Title: Study of cooperative dislocation phenomena in solids by the acoustic emis- sion technique Author: Michal KNAPEK Department: Department of Physics of Materials Supervisor: doc. RNDr. František Chmelík, CSc., Department of Physics of Materials Abstract: Plastic deformation of micron-scale crystalline materials differs con- siderably from bulk specimens, as it is characterized by random strain bursts. Three categories of metallic samples were investigated in this thesis: micron- scale copper micropillars with varied geometries, submillimeter-scale aluminum microwires, and aluminum and aluminum-magnesium salt-replicated foams. Very precise fabrication methods and sensitive measurement set-ups consisting of uni- axial compression and tensile tests with concurrent acoustic emission (AE) record- ing were developed. These fine methods allowed for investigations of effects re- lated to plastic deformation at micrometer scales, i.e. the dislocation dynamics associated with the stress drops. Size effects in plastic deformation, as well as clear correlations between the stress drops and the AE events, were found in mi- crosamples, confirming that dislocation avalanches are indeed responsible for the stochastic character of deformation processes also at microscales. Open-cell pure aluminum and aluminum-magnesium...
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Study of cooperative dislocation phenomena in solids by the acoustic emission technique
Knapek, Michal ; Chmelík, František (advisor)
Title: Study of cooperative dislocation phenomena in solids by the acoustic emis- sion technique Author: Michal KNAPEK Department: Department of Physics of Materials Supervisor: doc. RNDr. František Chmelík, CSc., Department of Physics of Materials Abstract: Plastic deformation of micron-scale crystalline materials differs con- siderably from bulk specimens, as it is characterized by random strain bursts. Three categories of metallic samples were investigated in this thesis: micron- scale copper micropillars with varied geometries, submillimeter-scale aluminum microwires, and aluminum and aluminum-magnesium salt-replicated foams. Very precise fabrication methods and sensitive measurement set-ups consisting of uni- axial compression and tensile tests with concurrent acoustic emission (AE) record- ing were developed. These fine methods allowed for investigations of effects re- lated to plastic deformation at micrometer scales, i.e. the dislocation dynamics associated with the stress drops. Size effects in plastic deformation, as well as clear correlations between the stress drops and the AE events, were found in mi- crosamples, confirming that dislocation avalanches are indeed responsible for the stochastic character of deformation processes also at microscales. Open-cell pure aluminum and aluminum-magnesium...
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